International Journal of

ADVANCED AND APPLIED SCIENCES

EISSN: 2313-3724, Print ISSN: 2313-626X

Frequency: 12

line decor
  
line decor

 Volume 9, Issue 9 (September 2022), Pages: 33-40

----------------------------------------------

 Original Research Paper

 Fabrication and characterization of nanostructured Fe–28Mn–6Si–5Cr shape memory alloy

 Author(s): A. Syed Bava Bakrudeen 1, D. Jeyasimman 1, *, A. Balaji 2

 Affiliation(s):

 1Department of Mechanical Engineering, Periyar Maniammai Institute of Science and Technology, Vallam, India
 2Department of Mechanical Engineering, Al Ameen Engineering College, Erode, India

  Full Text - PDF          XML

 * Corresponding Author. 

  Corresponding author's ORCID profile: https://orcid.org/0000-0002-0780-9609

 Digital Object Identifier: 

 https://doi.org/10.21833/ijaas.2022.09.005

 Abstract:

Mechanical alloying and consequent sintering techniques were used to create a bulk alloy of Fe–28Mn–6Si–5Cr from elemental powder. The microstructure and shape memory behavior due to bending deformation were investigated. The majority of α phases that existed at the start of the mechanical alloying process were changed into γ phases by the end of the 40-hour process. The γ phase was essential to achieving shape recovery behavior, which was boosted by mechanical alloying. A stress-induced γ to ε phase transformation occurred at the end of the bending deformation process. Shape recovery was observed after the subsequent heat treatment process due to reverse martensitic ε to γ phase transformation. After mechanical alloying, a grain size of 9.5 nm was attained and a considerable amount of shape recovery was achieved at the end of the recovery heat-treatment process. As a result, we came to the conclusion that combining mechanical alloying with powder metallurgy and then sintering has the potential to synthesize Fe-Mn-Si-Cr shape memory alloy.

 © 2022 The Authors. Published by IASE.

 This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).

 Keywords: Shape memory alloy, Shape memory effect, Mechanical alloying

 Article History: Received 18 January 2022, Received in revised form 12 April 2022, Accepted 31 May 2022

 Acknowledgment 

No Acknowledgment.

 Compliance with ethical standards

 Conflict of interest: The author(s) declared no potential conflicts of interest with respect to the research, authorship, and/or publication of this article.

 Citation:

 Bakrudeen ASB, Jeyasimman D, and Balaji A (2022). Fabrication and characterization of nanostructured Fe–28Mn–6Si–5Cr shape memory alloy. International Journal of Advanced and Applied Sciences, 9(9): 33-40

 Permanent Link to this page

 Figures

 Fig. 1 Fig. 2 Fig. 3 Fig. 4 Fig. 5 Fig. 6 Fig. 7 Fig. 8

 Tables

 Table 1 Table 2

----------------------------------------------    

 References (25)

  1. Bakrudeen A, Jeyasimman D, and Balaji A (2022). Effect of compaction pressure, sintering temperature and recovery heat treatment temperature of powder metallurgical Fe-20Mn-5Si-5Ni-8Cr shape memory alloy. MRS Advances, 7(10): 222-228. https://doi.org/10.1557/s43580-022-00247-w   [Google Scholar]
  2. Cao B and Iwamoto T (2019). An experimental investigation on rate dependency of thermomechanical and stress-induced martensitic transformation behavior in Fe-28Mn-6Si-5Cr shape memory alloy under compression. International Journal of Impact Engineering, 132: 103284. https://doi.org/10.1016/j.ijimpeng.2019.04.026   [Google Scholar]
  3. Dogan A and Arslan H (2012). Effect of ball-milling conditions on microstructure during production of Fe–20Mn–6Si–9Cr shape memory alloy powders by mechanical alloying. Journal of Thermal Analysis and Calorimetry, 109(2): 933-938. https://doi.org/10.1007/s10973-011-1809-x   [Google Scholar]
  4. Druker A, Vermaut P, and Malarría J (2018). The shape recovery conditions for Fe–Mn–Si alloys: an interplay between martensitic transformation and plasticity. Materials Characterization, 139: 319-327. https://doi.org/10.1016/j.matchar.2018.03.018   [Google Scholar]
  5. Jeyasimman D, Narayanasamy R, and Ponalagusamy R (2015). Role of hybrid reinforcement on microstructural observation, characterization and consolidation behavior of AA 6061 nanocomposite. Advanced Powder Technology, 26(4): 1171-1182. https://doi.org/10.1016/j.apt.2015.05.013   [Google Scholar]
  6. Jeyasimman D, Sivaprasad K, Sivasankaran S, and Narayanasamy R (2014b). Fabrication and consolidation behavior of Al 6061 nanocomposite powders reinforced by multi-walled carbon nanotubes. Powder Technology, 258: 189-197. https://doi.org/10.1016/j.powtec.2014.03.039   [Google Scholar]
  7. Jeyasimman D, Sivasankaran S, Sivaprasad K, Narayanasamy R, and Kambali RS (2014a). An investigation of the synthesis, consolidation and mechanical behaviour of Al 6061 nanocomposites reinforced by TiC via mechanical alloying. Materials and Design, 57: 394-404. https://doi.org/10.1016/j.matdes.2013.12.067   [Google Scholar]
  8. Kim YS, Choi E, and Kim WJ (2018). Characterization of the microstructures and the shape memory properties of the Fe-Mn-Si-Cr-Ni-C shape memory alloy after severe plastic deformation by differential speed rolling and subsequent annealing. Materials Characterization, 136: 12-19. https://doi.org/10.1016/j.matchar.2017.11.055   [Google Scholar]
  9. Kong J, Song X, Shao X, Liu X, and Feng S (2018). The preparation, formation mechanism and magnetic properties of a Fe-Cr-Mn-N amorphous alloy. Advanced Powder Technology, 29(12): 3348-3356. https://doi.org/10.1016/j.apt.2018.09.013   [Google Scholar]
  10. Kursun C and Gogebakan M (2015). Characterization of nanostructured Mg–Cu–Ni powders prepared by mechanical alloying. Journal of Alloys and Compounds, 619: 138-144. https://doi.org/10.1016/j.jallcom.2014.08.126   [Google Scholar]
  11. Li H, Yin F, Sawaguchi T, Ogawa K, Zhao X, and Tsuzaki K (2008). Texture evolution analysis of warm-rolled Fe–28Mn–6Si–5Cr shape memory alloy. Materials Science and Engineering: A, 494(1-2): 217-226. https://doi.org/10.1016/j.msea.2008.05.013   [Google Scholar]
  12. Liu J and Chen W (2018). Microstructure and mechanical properties of a spark plasma sintered Fe-11Cr-2.3 B-6Al-15Mn alloy. Vacuum, 150: 49-57. https://doi.org/10.1016/j.vacuum.2018.01.029   [Google Scholar]
  13. Liu X, Cheng H, Li Z, Wang H, Chang F, Wang W, and Dai P (2019). Microstructure and mechanical properties of FeCoCrNiMnTi0. 1C0. 1 high-entropy alloy produced by mechanical alloying and vacuum hot pressing sintering. Vacuum, 165: 297-304. https://doi.org/10.1016/j.vacuum.2019.04.043   [Google Scholar]
  14. Lü L and Lai MO (1997). Mechanical alloying. Springer Science and Business Media, Berlin, Germany.   [Google Scholar]
  15. Maji BC, Krishnan M, and Ray RK (2011). Role of Si in improving the shape recovery of FeMnSiCrNi shape memory alloys. Metallurgical and Materials Transactions A, 42(8): 2153-2165. https://doi.org/10.1007/s11661-011-0651-x   [Google Scholar]
  16. Nespoli A, Villa E, and Passaretti F (2019). Effect of annealing on the microstructure of Yttrium-doped NiTiCu shape memory alloys. Journal of Alloys and Compounds, 779: 30-40. https://doi.org/10.1016/j.jallcom.2018.11.228   [Google Scholar]
  17. Otsuka H, Yamada H, Maruyama T, Tanahashi H, Matsuda S, and Murakami M (1990). Effects of alloying additions on Fe-Mn-Si shape memory alloys. The Iron and Steel Institute of Japan (ISIJ) International, 30(8): 674-679. https://doi.org/10.2355/isijinternational.30.674   [Google Scholar]
  18. Paleu V, Gurău G, Comăneci RI, Sampath V, Gurău C, and Bujoreanu LG (2018). A new application of Fe-28Mn-6Si-5Cr (mass%) shape memory alloy, for self-adjustable axial preloading of ball bearings. Smart Materials and Structures, 27(7): 075026. https://doi.org/10.1088/1361-665X/aac4c5   [Google Scholar]
  19. Sivasankaran S, Sivaprasad K, Narayanasamy R, and Iyer VK (2010). An investigation on flowability and compressibility of AA 6061100−x-x wt.% TiO2 micro and nanocomposite powder prepared by blending and mechanical alloying. Powder Technology, 201(1): 70-82. https://doi.org/10.1016/j.powtec.2010.03.013   [Google Scholar]
  20. Suryanarayana C (2001). Mechanical alloying and milling. Progress in Materials Science, 46(1-2): 1-184. https://doi.org/10.1016/S0079-6425(99)00010-9   [Google Scholar]
  21. Velmurugan C, Senthilkumar V, Biswas K, and Yadav S (2018). Densification and microstructural evolution of spark plasma sintered NiTi shape memory alloy. Advanced Powder Technology, 29(10): 2456-2462. https://doi.org/10.1016/j.apt.2018.06.026   [Google Scholar]
  22. Xu Z, Hodgson MA, and Cao P (2015). A comparative study of powder metallurgical (PM) and wrought Fe–Mn–Si alloys. Materials Science and Engineering: A, 630: 116-124. https://doi.org/10.1016/j.msea.2015.02.021   [Google Scholar]
  23. Xu Z, Hodgson MA, and Cao P (2016a). Effect of immersion in simulated body fluid on the mechanical properties and biocompatibility of sintered Fe–Mn-based alloys. Metals, 6(12): 309. https://doi.org/10.3390/met6120309   [Google Scholar]
  24. Xu Z, Hodgson MA, and Cao P (2016b). Effects of mechanical milling and sintering temperature on the densification, microstructure and tensile properties of the Fe–Mn–Si powder compacts. Journal of Materials Science and Technology, 32(11): 1161-1170. https://doi.org/10.1016/j.jmst.2016.08.024   [Google Scholar]
  25. Xu Z, Hodgson MA, Chang K, Chen G, Yuan X, and Cao P (2017). Effect of sintering time on the densification, microstructure, weight loss and tensile properties of a powder metallurgical Fe-Mn-Si alloy. Metals, 7(3): 81. https://doi.org/10.3390/met7030081   [Google Scholar]